Sodium Methoxide → HCID 21323434, compound

HRID 26527Notes

Reaction equation

HRID 26527 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[CH2:11][C:10]3=[N:12][N:13]=[C:14](S(C)(=O)=O)[N:9]3[CH:8]=[CH:7][C:6]=2[CH:19]=1.[CH3:20][O-:21].[Na+]>>[CH3:20][O:21][C:14]1[N:9]2[C:10]([CH2:11][C:5]3[CH:4]=[CH:3][C:2]([CH3:1])=[CH:19][C:6]=3[CH:7]=[CH:8]2)=[N:12][N:13]=1

Participants

3

Reactant 2

HCID 10942334Sodium MethoxideHCID 21323360HCID 21323360, compound

Product 1

HCID 21323434HCID 21323434, compound

Procedure

The reaction of 8-methyl-3-methylsulfonyl-11H-s-triazolo[3,4-b][3]benzazepine with sodium methoxide yielded 3-methoxy-8-methyl-11H-s-triazolo[3,4-b][3]benzazepine. Colorless prisms (as recrystallized from ethyl acetate), melting point: 148°-149° C.

Sources & evidence

ORD record
ord-a4361762a7d1436294aad49e225cb433
Source dataset
uspto-grants-1979_04
Patent number
US04150139

Reaction notes

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