HuagongsheHuagongshe Chemistry Print Report · For research reference only
Beta-Alanine → 2-[2-Phenylethoxy]ethylidene propanedinitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Beta-Alanine | HCID 239 | — |
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | Acetaldehyde, 2-(2-phenylethoxy)- | HCID 162493 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-[2-Phenylethoxy]ethylidene propanedinitrile | HCID 19082226 | 56.6% |
Reaction Steps
β-Alanine (0.6 g) was added to a solution of [2-phenylethoxy]acetaldehyde (8.0 g) and malononitrile (3.5 g) in ethanol (100 ml). The mixture was stirred at room temperature for 3 hours. The solid was filtered off, washed with fresh ethanol and dried to yield the subtitled compound (5.85g, 54%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648370 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-5793815e14e441d29c427bd2039acbce |
| Source note | uspto-grants-1997_07 |