m-Chloroperbenzoic acid → HCID 86751075, compound

Participants

Reaction Steps

By proceeding in accordance with the method of operation described in Example 2, starting from 2.14 g (5.6 mmol) of the crude compound obtained in Example 3 and 1.93 g (11.2 mmol) of 72% 3-chloroperbenzoic acid in 55 ml of dichloromethane, 0.9 g (2.26 mmol) of a mixture of the two expected diastereoisomers (73/27) is obtained in the form of a mousse after chromatography on silica gel twice (eluant: hexane/ethyl acetate, 3:1).

Provenance & Evidence