HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 8-bromooctanoate → HCID 22916408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 8-bromooctanoate | HCID 264813 | — |
| Reactant | HCID 4148530 | HCID 4148530 | — |
| Product | HCID 22916408 | HCID 22916408 | 99.4% |
Reaction Steps
2-(4-Octyloxyphenyl)-4,5-diphenylimidazole (2.5 g) was reacted with ethyl 8-bromooctanoate (2.96 g) in a method similar to Example 9. Column chromatography on silica gel eluted with a hexane:ethyl acetate gradient gave 1-(7-ethoxycarbonylheptyl)-2-[4-octyloxyphenyl]-4,5-diphenylimidazole (3.48 g, 94%) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648373 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-b527955566b6452c9f7b50c17f82386e |
| Source note | uspto-grants-1997_07 |