Potassium Carbonate → HCID 10479124, compound

Participants

Reaction Steps

A mixture of 1,4,5 triphenylimidazole (6.24 g), ethyl 6-bromohexanoate (13.38 g), potassium carbonate (13.2 g) and 2-butanone was stirred at reflux for 6 hours. The mixture was filtered, and the filtrate was evaporated. The residue was chromatographed on silica gel eluted with ethanol-hexane to give the title compound (5.61 g) m.p. 104°-106° C. Found: C, 76.35; H, 6.58; N, 6.07%; (C29H30N2O2O3) Requires: C, 76.63; H, 6.65; N, 6.16%

Provenance & Evidence