HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic acid, ethyl ester → Methyl 2-[(ethoxycarbonyl)amino]-1-cycloheptene-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic acid, ethyl ester | HCID 5641 | — |
| Reactant | Methyl 2-oxocycloheptane-1-carboxylate | HCID 288225 | — |
| Product | Methyl 2-[(ethoxycarbonyl)amino]-1-cycloheptene-1-carboxylate | HCID 53887984 | — |
Reaction Steps
Using the method of Example 1 Part A, methyl 2-oxocycloheptanecarboxylate (50.5 g, 0.30 mole) was reacted with urethane to provide 59 g of methyl 2-[(ethoxycarbonyl)amino]-1-cycloheptene-1-carboxylate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648516 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-148a294c988e417ab525a4f8902eccb1 |
| Source note | uspto-grants-1997_07 |