HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86751088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86751086 | HCID 86751086 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86751088 | HCID 86751088 | 83.2% |
Reaction Steps
A solution of 17-3 (45 mg, 0.10 mmol), TFA (1 mL), and CH2Cl2 (1 mL) was stirred at ambient temperature for 1.0 h. Concentration and flash chromatography (silica, 10:1:1 ethanol H2O/NH4OH) gave 17-4 (28 mg) as a white solid. Rf 0.17 (10:1:1 ethanol) H2O/NH4OH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648368 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-d2291c24500e42eba570feccb881fe17 |
| Source note | uspto-grants-1997_07 |