Tetrahydrofuran → HCID 70081150, compound

Participants

Reaction Steps

A solution of 25-2 (4.6 g, 18.8 mmol) in THF (50 mL) at ambient temperature was treated dropwise with LiAlH4 (9.4 mL, 9.4 mmol, 1M in THF). After stirring for 1 hour the reaction was quenched with a saturated sodium potassium tartrate solution. The mixture was then poured into EtOAc and washed with H2O and brine, dried (MgSO4) and concentrated to yield 25-3 as a yellow oil.

Provenance & Evidence