HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenylpiperidine-4-carboxamide monohydrochloride → HCID 54265877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenylpiperidine-4-carboxamide monohydrochloride | HCID 3017129 | — |
| Reactant | 2-[3-(3,4-Dichloro-phenyl)-5-oxo-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate | HCID 86750925 | — |
| Product | HCID 54265877 | HCID 54265877 | — |
Reaction Steps
Prepare according to the method of example 3.3 using 2-[3-(3,4-dichloro-phenyl)-5-oxo-1-(3,4,5-trimethoxy-benzoyl)-pyrrolidin-3-yl]-ethyl-methanesulfonate (5 mmol) and 4-phenyl-piperidine-4-carboxylic acid amide hydrochloride (7.5 mmol, 1.5 eq.). Chromatograph on silica gel to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05648366 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-bc0bf51d97df48439e4e1aaceb7852b8 |
| Source note | uspto-grants-1997_07 |