3,4-Difluorophenol → HCID 178444228, compound

HRID 265988Notes

Reaction equation

HRID 265988 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[CH:6][C:7]=1[F:8].[CH2:10]([Si:17]1(C2C=CC=CC=2)[CH2:22][CH2:21][CH:20]([C:23](O)=[O:24])[CH2:19][CH2:18]1)[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>>[CH2:10]([Si@H:17]1[CH2:18][CH2:19][C@H:20]([C:23]([O:9][C:4]2[CH:5]=[CH:6][C:7]([F:8])=[C:2]([F:1])[CH:3]=2)=[O:24])[CH2:21][CH2:22]1)[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 759273,4-DifluorophenolHCID 190321564-n-Heptyl-4-phenyl-4-silacyclohexanecarboxylic acid

Product 1

HCID 178444228HCID 178444228, compound

Procedure

The general procedure of Example 3 was repeated using 3,4-difluorophenol and 4-n-heptyl-4-phenyl-4-silacyclohexanecarboxylic acid, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-1d50a264ea3242fcb687b2c7515adfe4
Source dataset
uspto-grants-1997_07
Patent number
US05650092

Reaction notes

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