3-Fluoro-4-(trifluoromethoxy)phenol → HCID 178444230, compound

HRID 265990Notes

Reaction equation

HRID 265990 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:13])[CH:5]=[CH:6][C:7]=1[O:8][C:9]([F:12])([F:11])[F:10].[CH2:14]([Si:21]1(C2C=CC=CC=2)[CH2:26][CH2:25][CH:24]([C:27](O)=[O:28])[CH2:23][CH2:22]1)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]>>[CH2:14]([Si@H:21]1[CH2:22][CH2:23][C@H:24]([C:27]([O:13][C:4]2[CH:5]=[CH:6][C:7]([O:8][C:9]([F:11])([F:12])[F:10])=[C:2]([F:1])[CH:3]=2)=[O:28])[CH2:25][CH2:26]1)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 27833573-Fluoro-4-(trifluoromethoxy)phenolHCID 190321564-n-Heptyl-4-phenyl-4-silacyclohexanecarboxylic acid

Product 1

HCID 178444230HCID 178444230, compound

Procedure

The general procedure of Example 3 was repeated using 3-fluoro-4-trifluoromethoxyphenol and 4-n-heptyl-4-phenyl-4-silacyclohexanecarboxylic acid, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-e9bc41273c584856be9521bf8229ca55
Source dataset
uspto-grants-1997_07
Patent number
US05650092

Reaction notes

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