3,4,5-Trifluorophenol → HCID 178444231, compound

HRID 265992Notes

Reaction equation

HRID 265992 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([F:9])[C:7]=1[F:8].[CH2:11]([Si:18]1(C2C=CC=CC=2)[CH2:23][CH2:22][CH:21]([C:24](O)=[O:25])[CH2:20][CH2:19]1)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17]>>[CH2:11]([Si@H:18]1[CH2:19][CH2:20][C@H:21]([C:24]([O:10][C:4]2[CH:3]=[C:2]([F:1])[C:7]([F:8])=[C:6]([F:9])[CH:5]=2)=[O:25])[CH2:22][CH2:23]1)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17]

Participants

3

Reactant 2

HCID 27779433,4,5-TrifluorophenolHCID 190321564-n-Heptyl-4-phenyl-4-silacyclohexanecarboxylic acid

Product 1

HCID 178444231HCID 178444231, compound

Procedure

The general procedure of Example 3 was repeated using 3,4,5-trifluorophenol and 4-n-heptyl-4-phenyl-4-silacyclohexanecarboxylic acid, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-57b4bc6bd2684905ad6e45577a649ab4
Source dataset
uspto-grants-1997_07
Patent number
US05650092

Reaction notes

Loading…