3,4-Difluorophenol → HCID 178461117, compound

HRID 265995Notes

Reaction equation

HRID 265995 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[CH:6][C:7]=1[F:8].[F:10][CH:11]([CH3:30])[CH2:12][CH2:13][CH2:14][Si:15]1(C2C=CC=CC=2)[CH2:20][CH2:19][CH:18]([C:21](O)=[O:22])[CH2:17][CH2:16]1>>[F:10][CH:11]([CH3:30])[CH2:12][CH2:13][CH2:14][Si@H:15]1[CH2:16][CH2:17][C@H:18]([C:21]([O:9][C:4]2[CH:5]=[CH:6][C:7]([F:8])=[C:2]([F:1])[CH:3]=2)=[O:22])[CH2:19][CH2:20]1

Participants

3

Reactant 2

HCID 759273,4-DifluorophenolHCID 19032158HCID 19032158, compound

Product 1

HCID 178461117HCID 178461117, compound

Procedure

The general procedure of Example 3 was repeated using (3,4-difluorophenol and 4-(4-fluoropentyl)-4-phenyl-4-silacyclohexanecarboxylic acid, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-2d87c16a56434e3ea54c284055f5b143
Source dataset
uspto-grants-1997_07
Patent number
US05650092

Reaction notes

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