Ethyl Acetate → HCID 86751102, compound

Participants

Reaction Steps

1-(1-[2-hydroxyethyl)piperazinyl-1,4-dimethylanthraquinone (1 mmol) is dissolved in CH2Cl2 (2 mL), and N-ethyldiisopropylamine (760 μL, 4 mmol) and N,N-diisopropylmethylphosphonamidic chloride (194 μL, 1 mmol) are added. After 30 min., the solution is poured into ethylacetate (5 mL, previously washed with 2×5 mL of 5% NaHCO3, and 2×5 mL of saturated NaCl). The ethylacetate phase is dried over Na2SO4 and evaporated to an oil, N-1,4-dimethylanthraquinonyl-O-methoxydiisopropylamino phosphite 1-(2-hydroxyethyl)piperazine.

Provenance & Evidence