HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hexyne → 1-(4-Bromophenyl) 2-heptyn-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hexyne | HCID 12732 | — |
| Reactant | 4-Bromobenzoyl chloride | HCID 68515 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 1-(4-Bromophenyl) 2-heptyn-1-one | HCID 54449136 | — |
Reaction Steps
The following were stirred at ambient temperature for about 2 hours 30 minutes, 49 ml of 1-hexyne, 75 ml of triethylamine, 40 mg of cuprous iodide, 40 mg of bis triphenylphosphine palladium dichloride and 9 g of parabromobenzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05650414 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-d3e7d920830c495f938c2d13386767bf |
| Source note | uspto-grants-1997_07 |