Ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoate → HCID 20386129, compound

HRID 26609Notes

Reaction equation

HRID 26609 reaction equation
[C:1]([C:4](C(OC(C)(C)C)=O)([CH2:19][CH2:20][CH2:21][CH:22]([O:28][C:29](=[O:31])[CH3:30])[CH2:23][O:24][CH2:25][CH2:26][CH3:27])[CH2:5][CH2:6][CH2:7][C:8]1[CH:18]=[CH:17][C:11]([C:12]([O:14][CH2:15][CH3:16])=[O:13])=[CH:10][CH:9]=1)(=[O:3])[CH3:2].C(C(CCCC(OC(=O)C)CCCCC)CCCC1C=CC(C(OCC)=O)=CC=1)(=O)C>>[C:1]([CH:4]([CH2:19][CH2:20][CH2:21][CH:22]([O:28][C:29](=[O:31])[CH3:30])[CH2:23][O:24][CH2:25][CH2:26][CH3:27])[CH2:5][CH2:6][CH2:7][C:8]1[CH:18]=[CH:17][C:11]([C:12]([O:14][CH2:15][CH3:16])=[O:13])=[CH:10][CH:9]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 20386101Ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoateHCID 20386132HCID 20386132, compound

Product 1

HCID 20386129HCID 20386129, compound

Procedure

This compound is prepared by the method described in Example 1, Step E, except that the product of Step B of the present example replaces ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoate. The title compound is purified by column chromatography on silica gel and is obtained as a yellowish, viscous oil.

Workup

  1. customThis compound is prepared by the method
  2. customThe title compound is purified by column chromatography on silica gel
  3. customis obtained as a yellowish, viscous oil

Sources & evidence

ORD record
ord-fb59a5e0848f4c17a0fc61149b59ba6a
Source dataset
uspto-grants-1979_04
Patent number
US04150235

Reaction notes

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