O-Benzylhydroxylamine → HCID 19032523, compound

HRID 266111Notes

Reaction equation

HRID 266111 reaction equation
O=[C:2]1[CH2:7][CH2:6][CH:5]([NH:8][C:9]2[CH:14]=[CH:13][N:12]=[C:11]([CH2:15][O:16][CH3:17])[C:10]=2[O:18][CH3:19])[CH2:4][CH2:3]1.[CH2:20]([O:27][NH2:28])[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[CH2:20]([O:27][N:28]=[C:2]1[CH2:7][CH2:6][CH:5]([NH:8][C:9]2[CH:14]=[CH:13][N:12]=[C:11]([CH2:15][O:16][CH3:17])[C:10]=2[O:18][CH3:19])[CH2:4][CH2:3]1)[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1

Participants

3

Reactant 2

HCID 102313O-BenzylhydroxylamineHCID 19032545HCID 19032545, compound

Product 1

HCID 19032523HCID 19032523, compound

Procedure

The synthesis was carried out analogously to Example 57 using 4-(4-oxocyclohexylamino)-3-methoxy-2-methoxymethylpyridine (Example 56) and O-benzylhydroxylamine.

Sources & evidence

ORD record
ord-f747d8509f884e93b28ea76eaabb772a
Source dataset
uspto-grants-1997_07
Patent number
US05650417

Reaction notes

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