HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 19032362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | Ethyl 2-chloromethyl-4-(3,4-dimethoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate | HCID 10813243 | — |
| Product | HCID 19032362 | HCID 19032362 | — |
Reaction Steps
According to the same manner as that described in Example 34, ethyl 2-chloromethyl-4-(3,4-dimethoxyphenyl)-6,7-dimethoxyquinoline-3-carboxylate was reacted with N-methylaniline to give ethyl 4-(3,4-dimethoxyphenyl)-2-(N-methyl-N-phenylaminomethyl)-6,7-dimethoxyquinoline-3-carboxylate. This compound was recrystallized from dichloromethane-hexane. Colorless prisms, mp. 194°-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05650410 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-bbadec305cb64a0f93bf3cadbd9ce9e9 |
| Source note | uspto-grants-1997_07 |