HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Edukt | Tridecanoic acid | HCID 12530 | — |
| Edukt | CID 11268547 | HCID 11268547 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 2-Dimethylaminopyridine | HCID 21885 | — |
Reaktionsschritte
Following a procedure similar to that described in Example 12, but using 400 mg of radicicol, 588 mg of tridecanoic acid, 6 ml of dry tetrahydrofuran, 566 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 688 mg of the title compound were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05650430 |
| Quelldatensatz | uspto-grants-1997_07 |
| ORD ID | ord-0760d9cd1d3649299511e003c9128795 |
| Quellennotiz | uspto-grants-1997_07 |