関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,7-Octadiene | HCID 19460 | — |
| 反応物 | Trichlorosilane | HCID 24811 | — |
| 生成物 | 7-Octenyltrichlorosilane | HCID 104122 | — |
| 生成物 | Octane-1,8-diylbis[trichlorosilane] | HCID 104123 | — |
反応手順
In another experiment, 220 g (1.62 mole) trichlorosilane was added slowly in 20 minutes to a stirred mixture of 660 g (6 mole) 1,7-octadiene at 35° C. Subsequently, the reaction mixture was heated at 50° C. for 24 hours to complete the addition and then fractionally distilled. This resulted in 322 g, i.e., 82%, 7-octenyl trichlorosilane and 24 g, i.e., 12%, 1,8-bis-trichlorosilyl octane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04151114 |
|---|
| 出典データセット | uspto-grants-1979_04 |
|---|
| ORD ID | ord-126e277b95434e16b751bd249a6511c6 |
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| 出典メモ | uspto-grants-1979_04 |
|---|
