HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphonoacetate → HCID 178473138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphonoacetate | HCID 13345 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Ethyl(ethoxychlorophosphinyl)acetate | HCID 12634156 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 178473138 | HCID 178473138 | — |
Reaction Steps
Ethyl(diethoxyphosphinyl)acetate (11.2 gm., 0.05 mol.) and phosphorus pentachloride (10.5 gm., 0.05 mol.) are dissolved in 200 ml. of benzene and refluxed overnight. The solvent is removed in vacuo, leaving yellow, oily, ethyl(ethoxychlorophosphinyl)acetate as residue (11.5 gm.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04151172 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-f5f7c881caa9453e8959c0b4ff68e9d8 |
| Source note | uspto-grants-1979_04 |