HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxyacetyl chloride → HCID 10597512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Reactant | 115661-42-2 | HCID 10854237 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10597512 | HCID 10597512 | — |
Reaction Steps
12 mmol of methoxyacetyl chloride are added to 12 mmol of 1-benzyl-4-[(3,4-dichlorophenyl)amino]piperidine obtained in the preceding stage in 50 ml of anhydrous tetrahydrofuran (THF). The mixture is brought to reflux for 3 hours. After cooling, the expected product is obtained by filtering the precipitate, which is washed with THF and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05652246 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-95c02b56a56c495b90db904c696b3a34 |
| Source note | uspto-grants-1997_07 |