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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 266845Generated: November 1, 2026

Sodium Bicarbonate → HCID 22168674, compound

https://huagongshe.com/reaction/266845

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 22168559HCID 22168559—
SolventMethanolHCID 887—
ProductHCID 22168674HCID 22168674—

Reaction Steps

Reduction of the above nitro compound by the method of Example 2, except that the solvent was methanol, and NaHCO3 solution was used to basify, gave allyl 2-allyloxy-5-aminobenzoate. Nmr (CDCl3): δ 3.23 (br, 2H); 4.53 (dt, 2H); 4.79 (d, 2H); 5.21-5.49 (m, 4H); 5.93-6.14 (m, 2H); 6.80 (m, 2H); 7.16 (d, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05652233
Source datasetuspto-grants-1997_07
ORD IDord-8f922fae21a340788be967779135e13d
Source noteuspto-grants-1997_07