HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 5-Allyl-5-(beta-carboethoxy-alpha-methyl-ethyl)-barbituric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | HCID 13023200 | HCID 13023200 | — |
| Product | 5-Allyl-5-(beta-carboethoxy-alpha-methyl-ethyl)-barbituric acid | HCID 13023201 | — |
Reaction Steps
5-(β-Carboethoxy-α-methyl-ethyl)-barbituric acid was treated with allyl bromide at 50° C. to afford 5-allyl-5-(β-carboethoxy-α-methyl-ethyl)-barbituric acid, m.p. 114°. Alkaline saponification of this compound afforded 5-allyl-5-(β-carboxy-α-methyl-ethyl)-barbituric acid, which was recrystallized from water, m.p. 200°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04151268 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-fcb3015fa3af46ecb23fab6c3a2b510a |
| Source note | uspto-grants-1979_04 |