Ethoxyacetyl chloride → N-(1'-methyl-2'-methoxyethyl)-N-ethoxyacetyl-2,6-dimethylaniline

Participants

Reaction Steps

With stirring, 7.3 g of ethoxyacetyl chloride in 20 ml of abs. toluene were added at room temperature to 9.6 g of N-(1'-methyl-2'-methoxyethyl)-2,6-dimethylaniline. After stirring for 3 hours at room temperature, the reaction mixture was filtered. The filtrate was freed from solvent and the residual oil was distilled in a high vacuum. Boiling point: 122°-124° C./0.04 torr.

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