Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 2,2-Dimethylphenethyl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 2,2-Dimethylphenethyl alcohol | HCID 70145267 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2,2-Dimethylphenethyl acetate | HCID 22906301 | — |
반응 단계
Dissolve 2,2-dimethylphenethyl alcohol (118.0 g, 0.786 mol) in pyridine (700 mL). Add, by dropwise addition, acetic anhydride (222 mL, 240.7 g, 2.358 mol) and stir overnight at room temperature. Evaporate the solvent in vacuo and purify by distillation to give the title compound as a clear colorless oil; bp 75° C. @ 0.4 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05652370 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-f8fdffdca91247c3a35178476078fe81 |
| 출처 메모 | uspto-grants-1997_07 |