HuagongsheHuagongshe Chemistry Print Report · For research reference only
N2 (benzyloxycarbonyl)-N1-isopentyl-L-prolinamide → HCID 57053150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N2 (benzyloxycarbonyl)-N1-isopentyl-L-prolinamide | HCID 86746219 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57053150 | HCID 57053150 | 111.5% |
Reaction Steps
A solution of 5.73 g of N2 -(benzyloxycarbonyl)-N1 -isopentyl-L-prolinamide in 600 ml of ethanol was hydrogenated over 0.8 g of 10% palladium-on-carbon catalyst for 3.75 hours. The catalyst was removed by filtration and the filtrate was evaporated to give 3.4 g of N1 -isopentyl-L-prolinamide as an oil which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05652369 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-43661b1651e143778e9b71bf14d20eb2 |
| Source note | uspto-grants-1997_07 |