HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 54289082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | Isobutyl chloroformate | HCID 62365 | — |
| Reactant | HCID 14036705 | HCID 14036705 | — |
| Product | HCID 54289082 | HCID 54289082 | — |
Reaction Steps
In a manner analogous to that described in Example 19(i), 7.70 g of N-(benzyloxycarbonyl)-3-(4-fluorophenyl)-DL-alanine were treated with isobutyl chloroformate followed by reaction with diazomethane to give 7.15 g of benzyl [2-(4-fluorophenyl)-1(RS)-(2-diazoacetyl)ethyl]carbamate as a yellow solid of melting point 97° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05652369 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-f054deabe5db4a948dca5c11383e9da4 |
| Source note | uspto-grants-1997_07 |