Hydrogen maleate → 2-Benzylamino-5-methyl-7-propylimidazo[5,1-f]-as-triazine

HRID 267199Notes

Reaction equation

[CH2:1]([NH:8][C:9]1[NH:14][CH2:13][C:12]2=[C:15]([CH3:21])[N:16]=[C:17]([CH2:18][CH2:19][CH3:20])[N:11]2[N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(O)(=O)/C=C\C([O-])=O>>[CH2:1]([NH:8][C:9]1[N:14]=[CH:13][C:12]2=[C:15]([CH3:21])[N:16]=[C:17]([CH2:18][CH2:19][CH3:20])[N:11]2[N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 11966254Hydrogen maleate

HCID 178440026HCID 178440026, compound

Product 1

HCID 543377282-Benzylamino-5-methyl-7-propylimidazo[5,1-f]-as-triazine

Procedure

2-Benzylamino-5-methyl-7-propylimidazo[5,1-f]-as-triazine was prepared from 2-benzylamino-3,4-dihydro-5-methyl-7-propylimidazo[5,1-f]-as-triazine (Example 12b). It was converted into its hydrogen maleate which had m.p. 141°-142°.

Sources & evidence

ORD record: ord-f1d1274bbeef4dc08fc42187edfe4513
Source dataset: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03941785

Reaction notes

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