Barbituric Acid → HCID 178440035, compound

HRID 267209Notes

Reaction equation

HRID 267209 reaction equation
[NH:1]1[C:8](=[O:9])[CH2:7][C:5](=[O:6])[NH:4][C:2]1=[O:3].[NH2:10][C:11]1[N:16]=[CH:15][C:14]2=[C:17]([CH3:23])[N:18]=[C:19]([CH2:20][CH2:21][CH3:22])[N:13]2[N:12]=1>O>[NH2:10][C:11]1[NH:16][CH:15]([CH:7]2[C:5](=[O:6])[NH:4][C:2](=[O:3])[NH:1][C:8]2=[O:9])[C:14]2=[C:17]([CH3:23])[N:18]=[C:19]([CH2:20][CH2:21][CH3:22])[N:13]2[N:12]=1

Participants

4

Reactant 2

HCID 6211Barbituric AcidHCID 12493505HCID 12493505, compound

Product 1

HCID 178440035HCID 178440035, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Barbituric acid (1.36 g.) and 2-amino-5-methyl-7-propylimidazo[5,1-f]-as-triazine (Example 4) (2 g.) in water (60 ml.) were stirred for 1.75 hours. The solid was collected and crystallised from water to give a solid m.p. 256°-258°.

Workup

  1. customThe solid was collected
  2. customcrystallised from water

Sources & evidence

ORD record
ord-9311256caec343ca8aa6bd24cb853980
Source dataset
uspto-grants-1976_03
Patent number
US03941785

Reaction notes

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