Dimedone → HCID 178440034, compound

HRID 267211Notes

Reaction equation

HRID 267211 reaction equation
[NH2:1][C:2]1[N:7]=[CH:6][C:5]2=[C:8]([CH3:14])[N:9]=[C:10]([CH2:11][CH2:12][CH3:13])[N:4]2[N:3]=1.[CH3:15][C:16]1([CH3:24])[CH2:21][C:20](=[O:22])[CH2:19][C:18](=[O:23])[CH2:17]1>C(O)C>[NH2:1][C:2]1[NH:7][CH:6]([CH:19]2[C:20](=[O:22])[CH2:21][C:16]([CH3:24])([CH3:15])[CH2:17][C:18]2=[O:23])[C:5]2=[C:8]([CH3:14])[N:9]=[C:10]([CH2:11][CH2:12][CH3:13])[N:4]2[N:3]=1

Participants

4

Reactant 2

HCID 31358DimedoneHCID 12493505HCID 12493505, compound

Product 1

HCID 178440034HCID 178440034, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

2-Amino-5-methyl-7-propylimidazo[5,1-f]-as-triazine (Example 4) (1 g.) in aqueous ethanol (20 ml., 1:1) and 5,5-dimethylcyclohexane-1,3-dione (1 g.) in aqueous ethanol (20 ml., 1:1) were mixed. The solid was collected and dried and had m.p. 243°.

Workup

  1. customThe solid was collected
  2. customdried

Sources & evidence

ORD record
ord-066e58b6bf104d2195e4d822894591c6
Source dataset
uspto-grants-1976_03
Patent number
US03941785

Reaction notes

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