反应详情

A mixture of 50 g. (0.372 mole) of 1-aminoindole, 50 g. (0.372 mole) of phenylacetone, 600 ml. of acetic acid and 50 g. of sodium acetate was heated for one hour on a steam bath. The precipitate which separated from the cooled mixture was collected and washed with isopropyl ether. The product melted at 145°C. The literature m.p. is 145°C., Chemical Abstracts 54, 19641 (1960).

1. additionA mixture of 50 g
2. customThe precipitate which separated from the cooled mixture
3. customwas collected
4. washwashed with isopropyl ether