反应详情

152 Mg of 3,4-methylenedioxy-benzyl alcohol, 500 mg of silver silicate and 30 ml of benzene were added to the flask described in Example II and the mixture was refluxed for 45 minutes and was then filtered to obtain 139 mg of 3,4-methylenedioxy-benzaldehyde melting at 36.8°C.

1. temperaturethe mixture was refluxed for 45 minutes
2. filtrationwas then filtered