4-Bromo-2,5-di(propan-2-yl)benzene-1-thiol → HCID 54452707, compound
Reaction equation
[Br:1][C:2]1[C:7]([CH:8]([CH2:10][CH3:11])[CH3:9])=[CH:6][C:5]([SH:12])=[C:4]([CH:13]([CH2:15][CH3:16])[CH3:14])[CH:3]=1.Br[C:18]1C(C(C)C)=CC(S)=C(C(C)C)C=1>>[CH3:18][S:12][C:5]1[CH:6]=[C:7]([CH:8]([CH2:10][CH3:11])[CH3:9])[C:2]([Br:1])=[CH:3][C:4]=1[CH:13]([CH2:15][CH3:16])[CH3:14]Participants
3
Procedure
4-Bromo-2,5-di-sec-butylphenyl methyl sulfide was prepared using the procedure of Example 1C except that 4-bromo-2,5-di-sec-butylbenzenethiol was substituted for the 4-bromo-2,5-diisopropylbenzenethiol. The resulting product had a boiling point of 126°C at 0.3 mm Hg.
Sources & evidence
- ORD record
- ord-601a2d6545b140b89ad2cb42eb2ef2ac
- Source dataset
- uspto-grants-1976_03
- Patent number
- US03941826
Reaction notes
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