HCID 21556733, compound → HCID 21556734, compound

HRID 267292Notes

Reaction equation

HRID 267292 reaction equation
[Cl:1][C:2]1[C:7]([CH:8]([CH3:10])[CH3:9])=[CH:6][C:5]([S:11](Cl)(=O)=O)=[C:4]([CH:15]([CH3:17])[CH3:16])[CH:3]=1.BrC1C(C(CC)C)=CC(S(Cl)(=O)=O)=C(C(CC)C)C=1>>[Cl:1][C:2]1[C:7]([CH:8]([CH3:9])[CH3:10])=[CH:6][C:5]([SH:11])=[C:4]([CH:15]([CH3:17])[CH3:16])[CH:3]=1

Participants

3

Reactant 2

HCID 21556733HCID 21556733, compoundHCID 21556738HCID 21556738, compound

Product 1

HCID 21556734HCID 21556734, compound

Procedure

4-Chloro-2,5-diisopropylbenzenethiol was prepared by the procedure of Example 2B except that 4-chloro-2,5-diisopropylbenzenesulfonyl chloride was substituted for the 4-bromo-2,5-di-sec-butylbenzenesulfonyl chloride. The resulting product had a boiling point of 93°-95°C at 0.3 mm Hg.

Sources & evidence

ORD record
ord-7bcc7dce0d8d41c4870e50af38de54c4
Source dataset
uspto-grants-1976_03
Patent number
US03941826

Reaction notes

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