Acetic Anhydride → HCID 54507813, compound

HRID 267327Notes

Reaction equation

[Cl:1][C:2]1[CH:24]=[CH:23][C:5]([CH:6]=[N:7][N:8]([CH3:22])[C:9]([N:11]([N:13]=[CH:14][C:15]2[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][CH:16]=2)[CH3:12])=[NH:10])=[CH:4][CH:3]=1.[C:25](OC(=O)C)(=[O:27])[CH3:26]>>[C:25]([N:10]=[C:9]([N:11]([N:13]=[CH:14][C:15]1[CH:16]=[CH:17][C:18]([Cl:21])=[CH:19][CH:20]=1)[CH3:12])[N:8]([N:7]=[CH:6][C:5]1[CH:23]=[CH:24][C:2]([Cl:1])=[CH:3][CH:4]=1)[CH3:22])(=[O:27])[CH3:26]

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 53851910HCID 53851910, compound

Product 1

HCID 54507813HCID 54507813, compound

Procedure

When 1,3-bis(p-chlorobenzylideneamino)-1,3-dimethylguanidine free base is submitted to the above reaction conditions with acetic anhydride, there is obtained the corresponding 2-acetyl-1,3-bis(4-chlorobenzylideneamino)-1,3-dimethylguanidine.

Sources & evidence

ORD record: ord-00c9dc2b417a4d6abe052c5f03257ce4
Source dataset: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03941825

Reaction notes

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