HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 178513179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | (4-Chlorobenzyl)hydrazine | HCID 3015209 | — |
| Reactant | HCID 178504058 | HCID 178504058 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178513179 | HCID 178513179 | — |
Reaction Steps
The same compound is synthesized by the reaction of equimolar quantities of p-chlorobenzylhydrazine and methyl-3-(4-chlorobenzylidene)thiocarbazimidate hydrochloride (see Example 10) in hot ethanol. It is also prepared by the reaction of equimolar amounts of 1-(p-chlorobenzyl)-S-methylisothiosemicarbazide and hydrazine in warm ethanol, which affords 1-amino-3-(p-chlorobenzylamino)guanidine, followed by treatment of the latter with an equimolar quantity of p-chlorobenzaldehyde in hot isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03941825 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-d32d94388db0458bbbed5df97ac5fcd2 |
| Source note | uspto-grants-1976_03 |