HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide → 2',5-Dichloro-2-[4-methyl-2-(phthalimidomethyl)imidazol-1-yl]benzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | HCID 21555827 | HCID 21555827 | — |
| Product | 2',5-Dichloro-2-[4-methyl-2-(phthalimidomethyl)imidazol-1-yl]benzophenone | HCID 21555825 | — |
Reaction Steps
In the manner given in Example 17, 2',5-dichloro-[2-(hydroxymethyl)-4-methylimidazol-1-yl]benzophenone is treated with phthalimide and triphenylphosphine and finally with diethyl azocarboxylate to give 2',5-dichloro-2-[4-methyl-2-(phthalimidomethyl)imidazol-1-yl]benzophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03941803 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-b2961df56fa14602a45592983c337a22 |
| Source note | uspto-grants-1976_03 |