Ethanol → HCID 21487185, compound

HRID 267451Notes

Reaction equation

HRID 267451 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=O)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[N:15]1C=C[N:17]=[C:16]1[CH2:20][N:21]1C(=O)C2=CC=CC=C2C1=O.NN.[CH2:35](O)[CH3:36]>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[N:15]2[CH:35]=[CH:36][N:17]=[C:16]2[CH2:20][N:21]=1

Participants

4

Reactant 3

HCID 702EthanolHCID 9321HydrazineHCID 21555880HCID 21555880, compound

Product 1

HCID 21487185HCID 21487185, compound

Procedure

In the manner given in Example 33, 2'-chloro-2-[2-(phthalimidomethyl)imidazol-1-yl]benzophenone in ethanol is heated with hydrazine to give 6-(o-chlorophenyl)-4H-imidazo[1,2-a][1,4]benzodiazepine.

Sources & evidence

ORD record
ord-775d6475fdef4fa7b0fdf820c6908e4a
Source dataset
uspto-grants-1976_03
Patent number
US03941803

Reaction notes

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