HCID 21527494, compound → HCID 21527499, compound

HRID 267471Notes

Reaction equation

HRID 267471 reaction equation
Cl[C:2]([N:14]=[C:15]=[O:16])([C:10](F)([F:12])[F:11])[C:3]([F:9])([F:8])[C:4]([F:7])([F:6])[Cl:5]>CCOCC.[Zn]>[F:11][C:10]([F:12])=[C:2]([N:14]=[C:15]=[O:16])[C:3]([F:8])([F:9])[C:4]([F:6])([F:7])[Cl:5]

Participants

4

Reactant 1

HCID 21527494HCID 21527494, compound

Product 1

HCID 21527499HCID 21527499, compound

Reagents, catalysts & solvents 2

HCID 23994ZincCatalystHCID 3283Diethyl EtherSolvent

Procedure

By the procedure of Example 2, adding 1,3-dichloro-1 -(trifluoromethyl)tetrafluoropropyl isocyanate to a suspension of powdered zinc in ether will yield 2,2-difluoro-1-(2-chlorotetrafluoroethyl)vinyl isocyanate.

Sources & evidence

ORD record
ord-578868cdc9644932a98d1d976be31311
Source dataset
uspto-grants-1976_03
Patent number
US03943112

Reaction notes

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