HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21434993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12801674 | HCID 12801674 | — |
| Product | HCID 21434993 | HCID 21434993 | — |
Reaction Steps
7-Chloro-1-ethyl-1,4-dihydro-4-oxo-1,8-naphthyridine-3-carboxylic acid (29.5 g) and thionyl chloride (18 ml) in dry doluene (900 ml) were stirred and heated under reflux for 1 hour. The solution was cooled and the solid that separated was collected. It had m.p. 186.5°-188.5° (98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03943141 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-697003830a5e49b69947b6b8479f6787 |
| Source note | uspto-grants-1976_03 |