HRID267526

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6858

Benzaldehyde, 3,4,5-trimethoxy-

C10H12O4

HCID66951

Diethyl 2-oxobutanedioate

C8H12O5

HCID643756

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)C1=C(C(=O)OCC)C(c2cc(OC)c(OC)c(OC)c2)C(C(=O)OCC)=C(C)N1

HCID68133689

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

11.8 g of 3,4,5-trimethoxybenzaldehyde, 14 g of oxalacetic acid diethyl ester and 7.8 g of β-aminocrotonic acid ethyl ester in 30 ccs of ethanol are heated to the boil overnight and light yellow crystals of melting point 134° are obtained.

WORKUP

后处理

customare obtained