HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzaldehyde → HCID 68127996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzaldehyde | HCID 11569 | — |
| Reactant | Diethyl oxalacetate | HCID 66951 | — |
| Reactant | 2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- | HCID 643756 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68127996 | HCID 68127996 | — |
Reaction Steps
27.2 g of 3-methoxybenzaldehyde, 38 g of oxalacetic acid diethyl ester and 26 g of β-aminocrotonic acid ethyl ester in 120 ccs of ethanol are heated to the boil overnight and evaporated in vacuo. Oil (orange).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03943140 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-186bbfb44e8143ec82c2580d78024fcf |
| Source note | uspto-grants-1976_03 |