Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 3-[(4-Dodecylbenzenesulfonamido)benzenesulfonyl]acrylonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 4-Dodecylbenzenesulfonyl chloride | HCID 104215 | — |
| 반응물 | 2-Cyanovinyl 4-aminophenyl sulfone | HCID 54561326 | — |
| 용매 | Acetate | HCID 175 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 3-[(4-Dodecylbenzenesulfonamido)benzenesulfonyl]acrylonitrile | HCID 54383505 | — |
반응 단계
6.9 grams (0.02 mol) of 4-dodecylbenzenesulfonyl chloride dissolved in 100 ml acetate are added, at room temperature, to a stirred solution of 3-(4-aminobenzenesulfonyl)acrylonitrile (4.2 g, 0.02 mol) and 3ml (0.02 mol) of triethylamine in 150 ml acetone. The mixture is permitted to stand overnight. 3-[(4-dodecylbenzenesulfonamido)benzenesulfonyl]acrylonitrile is recovered as a soft, fine yellow powder: ##SPC17##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03943154 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-e4f273a4111441fd921c2da30d7bc713 |
| 출처 메모 | uspto-grants-1976_03 |