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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 267628Generated: October 30, 2026

Citric Acid → HCID 131710093, compound

https://huagongshe.com/reaction/267628

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCitric AcidHCID 311—
ReactantHCID 22788260HCID 22788260—
SolventEthanolHCID 702—
ProductHCID 131710093HCID 13171009310%

Reaction Steps

A solution of 3α-hydroxy-17β-(2'-morpholinoethoxycarbonyl)-5β-androstan-11-one (112 mg., 0.25 mmole) in ethanol (2 ml.) was treated with 0.01 N aqueous citric acid (2.5 ml; 0.25 mmole) and the resulting mixture was evaporated to dryness. The residue was treated with water (1.1 ml) to give an aqueous solution of the title compound (10% with respect to free steroidal base).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03943124
Source datasetuspto-grants-1976_03
ORD IDord-389877487dba43be8a21289e95b57243
Source noteuspto-grants-1976_03