HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citric Acid → HCID 131710093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citric Acid | HCID 311 | — |
| Reactant | HCID 22788260 | HCID 22788260 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131710093 | HCID 131710093 | 10% |
Reaction Steps
A solution of 3α-hydroxy-17β-(2'-morpholinoethoxycarbonyl)-5β-androstan-11-one (112 mg., 0.25 mmole) in ethanol (2 ml.) was treated with 0.01 N aqueous citric acid (2.5 ml; 0.25 mmole) and the resulting mixture was evaporated to dryness. The residue was treated with water (1.1 ml) to give an aqueous solution of the title compound (10% with respect to free steroidal base).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03943124 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-389877487dba43be8a21289e95b57243 |
| Source note | uspto-grants-1976_03 |