HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → 3-(Chloromethoxy)-1,1,1,2,2-pentafluoropropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | Methyl 1H,1H-perfluoropropyl ether | HCID 2776015 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3-(Chloromethoxy)-1,1,1,2,2-pentafluoropropane | HCID 21517136 | — |
Reaction Steps
The ether V can be prepared by a method analogous to that described by Weinmayr1, or from methyl 2,2,3,3,3-pentafluoropropyl ether and one molar equivalent of sulfuryl chloride at 0°-35°C with ultraviolet irradiation to give the chloromethyl 2,2,3,3,3-pentafluoropropyl ether XXVII,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03943256 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-33b77c79906b47fab6b08d01596eb506 |
| Source note | uspto-grants-1976_03 |