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5-Bromovanillin → 5-Bromo-4-[(1,5-dimethyl-hexyl)-oxy]-m-anisaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Bromovanillin | HCID 18099 | — |
| 反応物 | 2-Bromo-6-methylheptane | HCID 138332 | — |
| 生成物 | 5-Bromo-4-[(1,5-dimethyl-hexyl)-oxy]-m-anisaldehyde | HCID 21487602 | — |
反応手順
2-bromo-6-methyl-heptane was reacted with 3-methoxy-4-hydroxy-5-bromo-benzaldehyde to obtain 5-bromo-4-[(1,5-dimethyl-hexyl)-oxy]-m-anisaldehyde (boiling point = 190°-193°C/0.1 mmHg); 2-bromo-6-methyl-heptane was reacted with p-hydroxy-benzonitrile to obtain p-[(1,5-dimethyl-hexyl)-oxy]-benzonitrile (boiling point = 165°-168°C/1.0 mmHg);
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03944531 |
| 出典データセット | uspto-grants-1976_03 |
| ORD ID | ord-addee749c944443b9a0ac796dff5d592 |
| 出典メモ | uspto-grants-1976_03 |