HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → HCID 4356499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | Benzeneacetonitrile, 4-methoxy- | HCID 66031 | — |
| Solvent | Sodium ethoxide | HCID 2723922 | — |
| Product | HCID 4356499 | HCID 4356499 | — |
Reaction Steps
Following the procedures outlined in Examples 1 and 3, p-methoxyphenylacetonitrile is reacted with diethyl oxalate in alcoholic sodium ethoxide solution to give ethyl 3-cyano-3-(p-methoxyphenyl)-pyruvate which is then similarly reacted with phenylacetonitrile to yield 2-(p-methoxyphenyl)-5-phenyl-3,4-dioxoadiponitrile, m.p. 256°-258° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03944571 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-24027d98674f43b29e31e71b85cd7326 |
| Source note | uspto-grants-1976_03 |