HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → HCID 19768834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | Benzeneacetonitrile, 4-fluoro- | HCID 68016 | — |
| Solvent | Sodium ethoxide | HCID 2723922 | — |
| Product | HCID 19768834 | HCID 19768834 | — |
Reaction Steps
By employing the procedures set forth in Examples 1 and 3, p-fluorophenylacetonitrile is reacted with diethyl oxalate in alcoholic sodium ethoxide to give ethyl 3-cyano-3-(p-fluorophenyl)-pyruvate. Reaction of the latter under similar conditions with p-fluorophenylacetonitrile results in 2,5-di-(p-fluorophenyl)-3,4-dioxoadiponitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03944571 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-3270820134c544cfab0dbd84d9b6bfcb |
| Source note | uspto-grants-1976_03 |