Methanesulfonyl chloride → HCID 68146779, compound

HRID 267781Notes

Reaction equation

[CH:1]([N:4]1[CH2:8][C:7]2([CH2:14][O:13][C:12]3[CH:15]=[CH:16][C:17]([NH2:19])=[CH:18][C:11]=3[O:10][CH2:9]2)[O:6][C:5]1=[O:20])([CH3:3])[CH3:2].[CH3:21][S:22](Cl)(=[O:24])=[O:23]>>[CH:1]([N:4]1[CH2:8][C:7]2([CH2:14][O:13][C:12]3[CH:15]=[CH:16][C:17]([NH:19][S:22]([CH3:21])(=[O:24])=[O:23])=[CH:18][C:11]=3[O:10][CH2:9]2)[O:6][C:5]1=[O:20])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 15557328HCID 15557328, compound

Product 1

HCID 68146779HCID 68146779, compound

Procedure

By reacting the oxazolidinone obtained in Step A with methanesulfonyl chloride and employing the other reaction conditions and procedure described in Example 87, Step A, there is obtained 3'-isopropyl-7-methanesulfonamido-3,4-dihydro-2H-1,5-benzodioxepin-3-spiro-5'-oxazolidin-2'-one.

Workup

customthe other reaction conditions and procedure

Sources & evidence

ORD record: ord-f8938f97b336406c84a07fde3c8be30c
Source dataset: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03944560

Reaction notes

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